Characterization of FTIR in Graphite from Palm Oil Waste with Ferric Chloride Catalyst
Indonesia has various sources of graphite in large quantities. One of them is palm oil waste. Palm oil is a horticultural crop that acts as the largest non-oil and gas foreign exchange contributor in Indonesia. This study aims to synthesize graphite from oil palm trunks with a catalyst through the pyrolysis method. This is an experimental research which eventually generated qualitative data to be analyzed. Oil palm trunks are dried in the sun, then crushed into powder with a grinder and sieved to 200 mesh. Graphite was synthesized using a carbonization step at 500°C. Impregnation using 3M ferric chloride (FeCl3), with a concentration variation of 10% and 30%. Further activation at a temperature of 900°C for 3 hours. The results synthesis of graphite powder were washed with hydrochloric acid (HCl) and distilled water repeatedly to obtain relatively pure graphite. Graphite characterization includes Fourier Transform Infrared Spectroscopy (FTIR). The results of FTIR analysis showed that graphite contains functional groups O–H, C–H, C–O, C?C, and C=C.
Allaberdiev, A. (2002). Application of FTIR for investigation of graphite materials.
Chung, D. D. L. (2002). Review: Graphite. In Journal of Materials Science (Vol. 37, Issue 8). https://doi.org/10.1023/A:1014915307738
Darmawan, D., Genua, V., Kristianto, S., & Hutubessy, J. I. B. (2021). Tanaman perkebunan prospektif Indonesia. Penerbit Qiara Media.
Dovbeshko, G. I., Chegel, V. I., Gridina, N. Y., Repnytska, O. P., Shirshov, Y. M., Tryndiak, V. P., Todor, I. M., & Solyanik, G. I. (2002). Surface enhanced IR absorption of nucleic acids from tumor cells: FTIR reflectance study. Biopolymers - Biospectroscopy Section, 67(6). https://doi.org/10.1002/bip.10165
Honorisal, M. B. P., Huda, N., Partuti, T., & Sholehah, A. (2020). Sintesis dan karakterisasi grafena oksida dari tempurung kelapa dengan metode sonikasi dan hidrotermal. Teknika: Jurnal Sains Dan Teknologi, 16(1). https://doi.org/10.36055/tjst.v16i1.7519
Kusumattaqiin, F., Ramli, R., Kurnyawaty, N., Halik, A., & Hira, T. (2020). Analisa struktur oksida grafena tereduksi. Dalton?: Jurnal Pendidikan Kimia Dan Ilmu Kimia, 3(1). https://doi.org/10.31602/dl.v3i1.3107
Mahmudah, F., & Kusumawati, D. H. (2020). Pengaruh penambahan katalis nikel terhadap homogenitas fasa dan konduktivitas listrik karbon dari serabut kelapa. Inovasi Fisika Indonesia, 9(2). https://doi.org/10.26740/ifi.v9n2.p119-124
Nandiyanto, A. B. D., Oktiani, R., & Ragadhita, R. (2019). How to read and interpret ftir spectroscope of organic material. Indonesian Journal of Science and Technology, 4(1). https://doi.org/10.17509/ijost.v4i1.15806
Ningrum, L. S., Haryani, S., & Supardi, K. I. (2020). Kajian Integrasi Nilai-Nilai Karakter Islami Peserta Didik dalam Materi Hidrokarbon di Sekolah Menegah Kejuruan. Jurnal Pendidikan Sains Indonesia, 8(2). https://doi.org/10.24815/jpsi.v8i2.15633
Perdani, F. P., Riyanto, C. A., & Martono, Y. (2021). Karakterisasi karbon aktif kulit singkong (manihot esculenta crantz) berdasarkan variasi konsentrasi H3PO4 dan lama waktu aktivasi. Indonesian Journal of Chemical Analysis (IJCA), 4(2), 72–81.
Saputri, L. H., & Sukmawan, R. (2020). Pengaruh Proses Blending dan Ultrasonikasi terhadap Struktur Morfologi Ekstrak Serat Limbah Batang Kelapa Sawit untuk Bahan Baku Bioplastik (Selulosa Asetat). Rekayasa, 13(1). https://doi.org/10.21107/rekayasa.v13i1.6180
Taufantri, Y., Irdhawati, I., & Asih, I. A. R. A. (2016). Sintesis dan Karakterisasi Grafena dengan Metode Reduksi Grafit Oksida Menggunakan Pereduksi Zn. Jurnal Kimia VALENSI, 2(1). https://doi.org/10.15408/jkv.v2i1.2233
Thebora, M. E., Kurnia Nastira Ningsih, & Muhammad Irhash Shalihin. (2020). Sintesis grafena dari limbah pelepah sawit (elaeis sp.) Dengan metode reduksi grafit oksida menggunakan pereduksi Zn. Jurnal Khazanah Intelektual, 3(2). https://doi.org/10.37250/newkiki.v3i2.48
Wachid, F. M., Perkasa, A. Y., Prasetya, F. A., Rosyidah, N., & Darminto. (2014). Synthesis and characterization of nanocrystalline graphite from coconut shell with heating process. AIP Conference Proceedings, 1586. https://doi.org/10.1063/1.4866759
Wulandari, R., Aritonang, H. F., & Wuntu, A. D. (2017). Sintesis dan Karakterisasi Nanografit. Chemistry Progress, 10(2).
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